Please use this identifier to cite or link to this item: https://hdl.handle.net/11147/5007
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dc.contributor.authorElçi, Latif-
dc.contributor.authorKolbe, Nina-
dc.contributor.authorElçi, Şükrü Gökhan-
dc.contributor.authorAndersson, Jan T.-
dc.date.accessioned2017-03-08T08:49:36Z-
dc.date.available2017-03-08T08:49:36Z-
dc.date.issued2011-07-15-
dc.identifier.citationElçi, L., Kolbe, N., Elçi, Ş. G., and Anderson, J.T. (2011). Solid phase extractive preconcentration coupled to gas chromatography- atomic emission detection for the determination of chlorophenols in water samples. Talanta, 85(1), 551-555. doi:10.1016/j.talanta.2011.04.028en_US
dc.identifier.issn0039-9140-
dc.identifier.issn0039-9140-
dc.identifier.issn1873-3573-
dc.identifier.urihttp://doi.org/10.1016/j.talanta.2011.04.028-
dc.identifier.urihttp://hdl.handle.net/11147/5007-
dc.description.abstractSolid-phase extraction (SPE) followed by derivatization and gas chromatography-atomic emission detection (GC-AED) was evaluated for the determination of five chlorophenols (CPs) in water samples. The derivatization was based on the esterification of phenolic compounds with ferrocenecarboxylic acid. The determination of the derivatized phenols was performed by GC-AED in the iron selective detection mode at 302 nm. The described method was tested on spiked water samples.The overall method gave detection limits of 1.6-3.7 ng L-1 and recoveries of 90.9-104.5% for the examined mono- to trichlorophenols in 10 mL water samples. The CPs extracted from a 10 mL water sample with SPE were concentrated into 100 μL of organic solvent, a preconcentration factor of 100. The method was applied to lake and tap water samples, and CP contents between 6 and 51 ng L-1 in lake water and between below the detection limit and 8 ng L-1 in tap water were found for different CPs. The method is quick, simple and gives excellent recoveries, limits of detection and standard deviations.en_US
dc.description.sponsorshipDeutscher Akademischer Austauschdienst (DAAD)en_US
dc.language.isoenen_US
dc.publisherElsevier Ltd.en_US
dc.relation.ispartofTalantaen_US
dc.rightsinfo:eu-repo/semantics/openAccessen_US
dc.subjectChlorophenolsen_US
dc.subjectDerivatizationen_US
dc.subjectFerrocenecarboxylic acid estersen_US
dc.subjectGC-AEDen_US
dc.subjectWater analysisen_US
dc.titleSolid phase extractive preconcentration coupled to gas chromatography- atomic emission detection for the determination of chlorophenols in water samplesen_US
dc.typeArticleen_US
dc.institutionauthorElçi, Şükrü Gökhan-
dc.departmentİzmir Institute of Technology. Chemistryen_US
dc.identifier.volume85en_US
dc.identifier.issue1en_US
dc.identifier.startpage551en_US
dc.identifier.endpage555en_US
dc.identifier.wosWOS:000292848900078en_US
dc.identifier.scopus2-s2.0-79958153283en_US
dc.relation.publicationcategoryMakale - Uluslararası Hakemli Dergi - Kurum Öğretim Elemanıen_US
dc.identifier.doi10.1016/j.talanta.2011.04.028-
dc.relation.doi10.1016/j.talanta.2011.04.028en_US
dc.coverage.doi10.1016/j.talanta.2011.04.028en_US
dc.identifier.wosqualityQ1-
dc.identifier.scopusqualityQ1-
item.openairecristypehttp://purl.org/coar/resource_type/c_18cf-
item.fulltextWith Fulltext-
item.openairetypeArticle-
item.languageiso639-1en-
item.cerifentitytypePublications-
item.grantfulltextopen-
Appears in Collections:Chemistry / Kimya
Scopus İndeksli Yayınlar Koleksiyonu / Scopus Indexed Publications Collection
WoS İndeksli Yayınlar Koleksiyonu / WoS Indexed Publications Collection
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