Please use this identifier to cite or link to this item:
https://hdl.handle.net/11147/5007
Full metadata record
DC Field | Value | Language |
---|---|---|
dc.contributor.author | Elçi, Latif | - |
dc.contributor.author | Kolbe, Nina | - |
dc.contributor.author | Elçi, Şükrü Gökhan | - |
dc.contributor.author | Andersson, Jan T. | - |
dc.date.accessioned | 2017-03-08T08:49:36Z | - |
dc.date.available | 2017-03-08T08:49:36Z | - |
dc.date.issued | 2011-07-15 | - |
dc.identifier.citation | Elçi, L., Kolbe, N., Elçi, Ş. G., and Anderson, J.T. (2011). Solid phase extractive preconcentration coupled to gas chromatography- atomic emission detection for the determination of chlorophenols in water samples. Talanta, 85(1), 551-555. doi:10.1016/j.talanta.2011.04.028 | en_US |
dc.identifier.issn | 0039-9140 | - |
dc.identifier.issn | 0039-9140 | - |
dc.identifier.issn | 1873-3573 | - |
dc.identifier.uri | http://doi.org/10.1016/j.talanta.2011.04.028 | - |
dc.identifier.uri | http://hdl.handle.net/11147/5007 | - |
dc.description.abstract | Solid-phase extraction (SPE) followed by derivatization and gas chromatography-atomic emission detection (GC-AED) was evaluated for the determination of five chlorophenols (CPs) in water samples. The derivatization was based on the esterification of phenolic compounds with ferrocenecarboxylic acid. The determination of the derivatized phenols was performed by GC-AED in the iron selective detection mode at 302 nm. The described method was tested on spiked water samples.The overall method gave detection limits of 1.6-3.7 ng L-1 and recoveries of 90.9-104.5% for the examined mono- to trichlorophenols in 10 mL water samples. The CPs extracted from a 10 mL water sample with SPE were concentrated into 100 μL of organic solvent, a preconcentration factor of 100. The method was applied to lake and tap water samples, and CP contents between 6 and 51 ng L-1 in lake water and between below the detection limit and 8 ng L-1 in tap water were found for different CPs. The method is quick, simple and gives excellent recoveries, limits of detection and standard deviations. | en_US |
dc.description.sponsorship | Deutscher Akademischer Austauschdienst (DAAD) | en_US |
dc.language.iso | en | en_US |
dc.publisher | Elsevier Ltd. | en_US |
dc.relation.ispartof | Talanta | en_US |
dc.rights | info:eu-repo/semantics/openAccess | en_US |
dc.subject | Chlorophenols | en_US |
dc.subject | Derivatization | en_US |
dc.subject | Ferrocenecarboxylic acid esters | en_US |
dc.subject | GC-AED | en_US |
dc.subject | Water analysis | en_US |
dc.title | Solid phase extractive preconcentration coupled to gas chromatography- atomic emission detection for the determination of chlorophenols in water samples | en_US |
dc.type | Article | en_US |
dc.institutionauthor | Elçi, Şükrü Gökhan | - |
dc.department | İzmir Institute of Technology. Chemistry | en_US |
dc.identifier.volume | 85 | en_US |
dc.identifier.issue | 1 | en_US |
dc.identifier.startpage | 551 | en_US |
dc.identifier.endpage | 555 | en_US |
dc.identifier.wos | WOS:000292848900078 | en_US |
dc.identifier.scopus | 2-s2.0-79958153283 | en_US |
dc.relation.publicationcategory | Makale - Uluslararası Hakemli Dergi - Kurum Öğretim Elemanı | en_US |
dc.identifier.doi | 10.1016/j.talanta.2011.04.028 | - |
dc.relation.doi | 10.1016/j.talanta.2011.04.028 | en_US |
dc.coverage.doi | 10.1016/j.talanta.2011.04.028 | en_US |
dc.identifier.wosquality | Q1 | - |
dc.identifier.scopusquality | Q1 | - |
item.openairecristype | http://purl.org/coar/resource_type/c_18cf | - |
item.fulltext | With Fulltext | - |
item.openairetype | Article | - |
item.languageiso639-1 | en | - |
item.cerifentitytype | Publications | - |
item.grantfulltext | open | - |
Appears in Collections: | Chemistry / Kimya Scopus İndeksli Yayınlar Koleksiyonu / Scopus Indexed Publications Collection WoS İndeksli Yayınlar Koleksiyonu / WoS Indexed Publications Collection |
CORE Recommender
SCOPUSTM
Citations
43
checked on Dec 6, 2024
WEB OF SCIENCETM
Citations
42
checked on Nov 23, 2024
Page view(s)
124
checked on Dec 2, 2024
Download(s)
266
checked on Dec 2, 2024
Google ScholarTM
Check
Altmetric
Items in GCRIS Repository are protected by copyright, with all rights reserved, unless otherwise indicated.