Please use this identifier to cite or link to this item: https://hdl.handle.net/11147/6297
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dc.contributor.authorÖlçer, Yekta Arya-
dc.contributor.authorDemirkurt, Merve-
dc.contributor.authorDemir, Mustafa Muammer-
dc.contributor.authorEroğlu, Ahmet Emin-
dc.date.accessioned2017-10-03T08:50:50Z-
dc.date.available2017-10-03T08:50:50Z-
dc.date.issued2017-
dc.identifier.citationÖlçer, Y. A., Demirkurt, M., Demir, M. M., and Eroğlu, A. E. (2017). Development of molecularly imprinted polymers (MIPs) as a solid phase extraction (SPE) sorbent for the determination of ibuprofen in water. RSC Advances, 7(50), 31441-31447. doi:10.1039/c7ra05254een_US
dc.identifier.issn2046-2069-
dc.identifier.urihttp://doi.org/10.1039/c7ra05254e-
dc.identifier.urihttp://hdl.handle.net/11147/6297-
dc.description.abstractIbuprofen is a well-known endocrine disrupter. In this study, highly selective molecularly imprinted polymers (MIPs) with different morphologies were synthesized via precipitation and bulk polymerization of methacrylic acid (MAA) and trimethylolpropane trimethacrylate (TRIM) in the presence of ibuprofen as a template. Non-imprinted polymers (NIPs) were also synthesized via the same procedure in the absence of ibuprofen. Spherical and monolithic MIPs were obtained using different experimental conditions, and the spherical MIP was shown to have better sorption towards ibuprofen. The optimum sample pH, sorbent amount, sample volume, and sorption time were determined to be 8.0, 25.0 mg, 10.0 mL, and 30.0 min, respectively. A methanol water mixture (MeOH:H2O, 80:20, pH 3.0) was employed as an eluent with >97% (±0.8, n = 3) desorption. The MIP demonstrated high selectivity towards ibuprofen in the presence of naproxen and ketoprofen. The validity of the proposed method was checked via spike recovery tests using drinking and tap water samples. The method worked efficiently for both water types, resulting in the recoveries of 97.2% (±0.3, n = 3) and 97.7% (±0.2, n = 3).en_US
dc.description.sponsorshipThe Scientific and Technological Research Council of Turkey (TUBITAK 114Z777)en_US
dc.language.isoenen_US
dc.publisherRoyal Society of Chemistryen_US
dc.relationinfo:eu-repo/grantAgreement/TUBITAK/KBAG/114Z777en_US
dc.relation.ispartofRSC Advancesen_US
dc.rightsinfo:eu-repo/semantics/openAccessen_US
dc.subjectEndocrine disruptersen_US
dc.subjectDrug productsen_US
dc.subjectMolecularly imprinted polymersen_US
dc.subjectBulk polymerizationen_US
dc.titleDevelopment of molecularly imprinted polymers (MIPs) as a solid phase extraction (SPE) sorbent for the determination of ibuprofen in wateren_US
dc.typeArticleen_US
dc.authoridTR130614en_US
dc.authoridTR8641en_US
dc.institutionauthorÖlçer, Yekta Arya-
dc.institutionauthorDemirkurt, Merve-
dc.institutionauthorDemir, Mustafa Muammer-
dc.institutionauthorEroğlu, Ahmet Emin-
dc.departmentİzmir Institute of Technology. Chemistryen_US
dc.departmentİzmir Institute of Technology. Materials Science and Engineeringen_US
dc.identifier.volume7en_US
dc.identifier.issue50en_US
dc.identifier.startpage31441en_US
dc.identifier.endpage31447en_US
dc.identifier.wosWOS:000404076400035en_US
dc.identifier.scopus2-s2.0-85021662789en_US
dc.relation.publicationcategoryMakale - Uluslararası Hakemli Dergi - Kurum Öğretim Elemanıen_US
dc.identifier.doi10.1039/c7ra05254e-
dc.relation.doi10.1039/c7ra05254een_US
dc.coverage.doi10.1039/c7ra05254een_US
dc.identifier.wosqualityQ2-
dc.identifier.scopusqualityQ1-
item.languageiso639-1en-
item.openairecristypehttp://purl.org/coar/resource_type/c_18cf-
item.cerifentitytypePublications-
item.grantfulltextopen-
item.fulltextWith Fulltext-
item.openairetypeArticle-
crisitem.author.dept03.09. Department of Materials Science and Engineering-
crisitem.author.dept04.01. Department of Chemistry-
Appears in Collections:Chemistry / Kimya
Materials Science and Engineering / Malzeme Bilimi ve Mühendisliği
Scopus İndeksli Yayınlar Koleksiyonu / Scopus Indexed Publications Collection
WoS İndeksli Yayınlar Koleksiyonu / WoS Indexed Publications Collection
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