Please use this identifier to cite or link to this item: https://hdl.handle.net/11147/6405
Title: Amalgamation performances of gold-coated quartz wool, alumina, silica, sand and carbon fiber for the determination of inorganic mercury in waters by cold vapor atomic absorption spectrometry
Authors: Erdem Şimşek, Arzu
Erdem Yayayürük, Aslı
Shahwan, Talal
Eroğlu, Ahmet Emin
Keywords: Amalgamation
Cold vapor atomic absorption spectrometry
Mercury concentrations
Preconcentration
Gold-coated sorbents
Publisher: Pleiades Publishing
Source: Erdem Şimşek, A., Erdem Yayayürük, A., Shahwan, T., and Eroğlu, A. E. (2017). Amalgamation performances of gold-coated quartz wool, alumina, silica, sand and carbon fiber for the determination of inorganic mercury in waters by cold vapor atomic absorption spectrometry. Journal of Analytical Chemistry, 72(5), 551-556. doi:10.1134/S1061934817050033
Abstract: Different gold-coated sorbents for amalgamation were applied for the determination of inorganic mercury in waters using a home-made cold vapor generation unit coupled to atomic absorption spectrometry. Among the gold-coated materials investigated (quartz wool, alumina, silica, sand and carbon fiber) quartz wool was found to give the most efficient results in terms of sorption and release. Analytical performance of the system without and with amalgamation was investigated and it was found that when amalgamation was applied, the linearity and slope of the calibration plots were independent on the sample volume for 1.0, 5.0 and 10.0 mL. Method validation was realized through the analysis of a sample of spring water spiked with 1.0 μg/L inorganic mercury and the spike recoveries were found to be 95 ± 1, 91 ± 3, and 99 ± 5% for 1.0, 5.0, and 10.0 mL, respectively. The results demonstrated that the methodology can be applied to these types of samples directly or after amalgamation, depending on the mercury concentration.
URI: http://doi.org/10.1134/S1061934817050033
http://hdl.handle.net/11147/6405
ISSN: 1061-9348
16083199
Appears in Collections:Chemistry / Kimya
Scopus İndeksli Yayınlar Koleksiyonu / Scopus Indexed Publications Collection
WoS İndeksli Yayınlar Koleksiyonu / WoS Indexed Publications Collection

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